1,2,3,6,7,8-六氢芘合成路线 (共 41 条)
反应条件
1: AlCl3 2: ZnCl2, NaCl / 320 °C View Scheme
参考文献
Clar,E. et al.
Tetrahedron, 1963 , vol. 19, p. 2185 - 2197
反应条件
1: AlCl3 / CH2Cl2 2: DDQ / benzene 3: 1.) POCl3 4: 48 percent / KOH / dioxane View Scheme
参考文献
Korshun; Manasova; Balakin; Malakhov; Perepelov; Sokolova; Berlin
Nucleosides and Nucleotides, 1998 , vol. 17, # 9-11 p. 1809 - 1812
反应条件
1: 1.) SnCl4, 2.) H2O / 1.) CH2Cl2, 0 deg C 2: 77 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / Heating View Scheme
参考文献
Bair; Andrews; Tuttle; Knick; Cory; McKee
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 1983 - 1990
反应条件
N-fluoro-2,4-dinitroimidazole in 1,2-dichloro-ethane 72 h; Heating;
参考文献
Laali, Kenneth K.; Tanaka, Mutsuo; Forohar, Farhad; Cheng, Michael; Fetzer, John C.
Journal of Fluorine Chemistry, 1998 , vol. 91, # 2 p. 185 - 190
反应条件
hydrogen; platinum in acetic acid T=25°C; P=760 Torr; 96 h; further conditions: Raney-Nickel, 300 deg C, 250 atm, cyclohexan; Product distribution;
参考文献
Mann, G.; Sicker, A.; Herzschuh, R.; Engewald, W.; Praefcke, K.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 267 - 272
反应条件
palladium on activated charcoal T=300°C;
参考文献
Lock; Walter
Chemische Berichte, 1944 , vol. 77/79, p. 286,292
反应条件
1: Br2 2: DDQ 3: (i) nBuLi, (ii) /BRN= 969135/ 4: (i) NBS, (PhCO)2O2, (ii) /BRN= 4652394/ 5: aq. KOH 6: HF 7: NaBH4 8: TsOH View Scheme
参考文献
Konieczny,M.; Harvey,R.G.
Journal of Organic Chemistry, 1979 , vol. 44, # 13 p. 2158 - 2160
反应条件
1: 94 percent / copper(II) nitrate trihydrate / acetic anhydride / 6 h / Ambient temperature 2: 92 percent / DDQ / nitrobenzene / 0.5 h / Heating View Scheme
参考文献
Bavin
Canadian Journal of Chemistry, 1959 , vol. 37, p. 1614
反应条件
1: Br2 2: DDQ 3: (i) nBuLi, (ii) /BRN= 969135/ View Scheme
参考文献
Hoeffinger,J.-P. et al.
Bulletin de la Societe Chimique de France, 1969 , p. 3099 - 3100
参考文献
Cook; Hewett
Journal of the Chemical Society, 1933 , p. 398,401
Chemistry and Industry (London, United Kingdom), 1936 , p. 843