二苯甲酮2,4-二硝基苯基腙合成路线 （共 19 条）
反应条件
sulfuric acid in methanol; water T=25°C;
参考文献
Lue, Ping; Fan, Wei-Qiang; Zhou, Xun-Jun
Synthesis, 1989 , # 9 p. 692 - 693
反应条件
iron (III) perchlorate in 1,2-dichloro-ethane T=20°C; 12 h;
参考文献
Oskooie, Hossien A.; Heravi, Majid M.; Sadnia, Akbar; Safarzadegan, Mehrak; Behbahani, Farahnaz K.
Mendeleev Communications, 2007 , vol. 17, # 3 p. 190 - 191
反应条件
1: 1,1,4-triphenylpenta-1,3-diene With potassium permanganate in acetone 0.5 h; Reflux; 2: (2,4-dinitro-phenyl)-hydrazine
参考文献
Ohta, Akihiro; Dahl, Klaus; Raab, Rainer; Geittner, Jochen; Huisgen, Rolf
Helvetica Chimica Acta, 2008 , vol. 91, # 5 p. 783 - 804
反应条件
1: pyridine 2: OsO4; diethyl ether; pyridine / Behandeln des Oxidationsprodukts mit wss. KOH und Mannit in CHCl3 und Behandeln des Reaktionsprodukts mit <2,4-Dinitro-phenyl>-hydrazin und wss.-aethanol. H2SO4 View Scheme
参考文献
Curtin; Hendrickson
Journal of Organic Chemistry, 1956 , vol. 21, p. 1260,1261,1263
反应条件
1: (1,2-epoxy-1-methylethyl)-benzene With hydrogenchloride; tetrafluoroboric acid diethyl ether complex; iodosylbenzene; palladium dichloride; Ba(OH)2 in diethyl ether; dichloromethane; water 7 h; Inert atmosphereMolecular sieve; 2: (2,4-dinitro-phenyl)-hydrazine Inert atmosphere;
参考文献
Havare, Nizam; Plattner, Dietmar A.
Helvetica Chimica Acta, 2012 , vol. 95, # 10 p. 2036 - 2042
参考文献
Busch; Kunder
Chemische Berichte, 1916 , vol. 49, p. 317
反应条件
diethyl ether; dinitrogen tetraoxide
参考文献
Busch; Kunder
Chemische Berichte, 1916 , vol. 49, p. 317
反应条件
pyridine; osmium(VIII) oxide; diethyl ether Behandeln des Oxidationsprodukts mit wss. KOH und Mannit in CHCl3 und Behandeln des Reaktionsprodukts mit <2,4-Dinitro-phenyl>-hydrazin und wss.-aethanol. H2SO4;
参考文献
Curtin; Hendrickson
Journal of Organic Chemistry, 1956 , vol. 21, p. 1260,1261,1263
反应条件
1: 1,1-di(phenyl)ethylene With tert.-butylhydroperoxide in benzene 1.5 h; 2: (2,4-dinitro-phenyl)-hydrazine in benzene
参考文献
Stepovik; Gulenova
Russian Journal of General Chemistry, 2009 , vol. 79, # 8 p. 1663 - 1670
反应条件
1: 74 percent / acetonitrile / 12 h / Ambient temperature 2: 1.) dibenzoyl peroxide, CCl4, 3 days, 2.) EtOH View Scheme
参考文献
Hadjiarapoglou, L.; Spyroudis, S.; Varvoglis, A.
Synthesis, 1983 , # 3 p. 207 - 208
