反应条件
1: 1) methyl iodide, Mg, iodine / 1a) 30 deg C, 5 h, 1b) overnight, 2a) gradually warmed to 30 deg C, 2b) 1.5 h, reflux, 2c) room temperature, overnight
2: 83 percent / 48percent HBr-CH3COOH, gl. acetic acid / 1) 6 h, 2) overnight, 30 deg C
View Scheme
参考文献
Rao, K. V. B.; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. <B> 19, # 6 p. 504 - 507
