4-溴-5-甲氧基-2-硝基苯胺合成路线 （共 9 条）
反应条件
1: With N-bromosuccinmide in acetonitrile T=0°C; 2: With trifluoroacetic acid in acetonitrile T=0 - 20°C; 24 h;
参考文献
Sheibani, Esmaeil; Waernmark, Kenneth
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 2059 - 2067
反应条件
hydrogenchloride; acetic acid 1 h; Heating;
参考文献
Kauffman; Litak; Boyko
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 5 p. 1541 - 1555
反应条件
1: H2 / 5percent Pd/C / ethyl acetate 3: KNO3 4: 10percent NaOH / ethanol / Heating View Scheme
参考文献
Zhou, Zhang-Lin; Weber, Eckard; Keana, John F. W.
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7583 - 7586
反应条件
1.1: methanol / 28 h / 20 °C / Inert atmosphere 2.1: N-bromosuccinmide / acetonitrile / 0 °C 2.2: 24 h / 0 - 20 °C View Scheme
参考文献
Sheibani, Esmaeil; Waernmark, Kenneth
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 2059 - 2067
反应条件
sodium hydroxide in ethanol Heating;
参考文献
Zhou, Zhang-Lin; Weber, Eckard; Keana, John F. W.
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7583 - 7586
反应条件
2: KNO3 3: 10percent NaOH / ethanol / Heating View Scheme
参考文献
Zhou, Zhang-Lin; Weber, Eckard; Keana, John F. W.
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7583 - 7586
反应条件
1: 62 percent / NaOAc, HOAc, Br2 / 0.5 h / 55 °C 2: 93 percent / 12 M HCl, acetic acid / 1 h / Heating View Scheme
参考文献
Kauffman; Litak; Boyko
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 5 p. 1541 - 1555
反应条件
1: 86 percent / 1 h / Heating 2: 46 percent / HNO3, Ac2O 3: 62 percent / NaOAc, HOAc, Br2 / 0.5 h / 55 °C 4: 93 percent / 12 M HCl, acetic acid / 1 h / Heating View Scheme
参考文献
Kauffman; Litak; Boyko
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 5 p. 1541 - 1555
反应条件
1: 46 percent / HNO3, Ac2O 2: 62 percent / NaOAc, HOAc, Br2 / 0.5 h / 55 °C 3: 93 percent / 12 M HCl, acetic acid / 1 h / Heating View Scheme
参考文献
Kauffman; Litak; Boyko
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 5 p. 1541 - 1555
