反应条件
1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C 2.1: triethylamine; hydrogen / palladium 10 on activated carbon / ethanol; water / 16 h / 3102.97 Torr 3.1: potassium hydroxide / water; tetrahydrofuran; methanol / 10 h / 0 °C 3.2: 10 h / 0 - 20 °C 4.1: triethylamine; 2-hydroxy-pyridine / 48 h / 90 °C 5.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C View Scheme
