1-甲基-2-羟甲基-1H-咪唑合成路线 (共 15 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; Reduction; 1 h;
参考文献
Hay, Michael P.; Wilson, William R.; Denny, William A.
Tetrahedron, 2000 , vol. 56, # 4 p. 645 - 657
反应条件
in acetonitrile T=120°C; 12 h;
参考文献
Liao, Chen; Shao, Nan; Han, Kee Sung; Sun, Xiao-Guang; Jiang, De-En; Hagaman, Edward W.; Dai, Sheng
Physical Chemistry Chemical Physics, 2011 , vol. 13, # 48 p. 21503 - 21510
反应条件
hydrogenchloride in formaldehyd; ethanol
参考文献
Merck and Co., Inc.
Patent: US4746669 A1, 1988 ;
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 79, p. 4922,4926
反应条件
sodium azide; sodium acetate; acetic acid in water; acetonitrile T=25°C; different NaCl concentration; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1139 - 1143
反应条件
sodium acetate; acetic acid in water 0.166667 h; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1139 - 1143
反应条件
thionyl chloride in diethyl ether; 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
THE UNIVERSITY OF MANCHESTER; ST GEORGE'S HOSPITAL MEDICAL SCHOOL
Patent: US2012/322722 A1, 2012 ;
反应条件
1: SOCl2 2: KCN; H2O 3: LiAlH4; diethyl ether View Scheme
参考文献
Journal of the Chemical Society, , p. 3305
反应条件
manganese(IV) oxide in chloroform 22 h; Ambient temperature;
参考文献
Santagostini, Laura; Gullotti, Michele; Pagliarin, Roberto; Bianchi, Emanuela; Casella, Luigi; Monzani, Enrico
Tetrahedron Asymmetry, 1999 , vol. 10, # 2 p. 281 - 295
参考文献
Grindley; Pyman
Journal of the Chemical Society, 1927 , p. 3132