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1: N,N-dimethyl-formamide; hydrogen; nitrogen; oxalyl dichloride / tetrahydrofuran / 2 h / 0 - 20 °C 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 1 h 3: 18-crown-6 ether; potassium methanolate / tetrahydrofuran / 0.25 h / 20 °C View Scheme

pyridine

diethyl ether

ruthenium(IV) oxide; sodium periodate 1) 5 h, room temp., pyridine; 2) acetic ester, water, 20 min : decomposition reaction;

ruthenium(IV) oxide; sodium periodate 1) 5 h, room temp., pyridine; 2) acetic ester, water, 20 min : decomposition reaction;

ruthenium(IV) oxide; sodium periodate 1) 5 h, room temp., pyridine; 2) acetic ester, water, 20 min : decomposition reaction;

ruthenium(IV) oxide; sodium periodate 1) 5 h, room temp., pyridine; 2) acetic ester, water, 20 min : decomposition reaction;