9H-吡啶并[3,4-b]吲哚-1-甲醇合成路线 （共 9 条）
反应条件
iron sulphate heptahydrate; dihydrogen peroxide in water T=10 - 15°C; Minisci reaction; 0.166667 h; regioselective reaction;
参考文献
Lin, Guowu; Wang, Yue; Zhou, Qingfa; Tang, Weifang; Wang, Jian; Lu, Tao
Synthetic Communications, 2011 , vol. 41, # 23 p. 3541 - 3550
反应条件
in methanol; water T=25°C; 5 h; +1.0V/30mA; anode: graphite felt, cathode: Pt, electrolyte: KH2PO4/K2HPO4;
参考文献
Bobbitt, James M.; Willis, John P.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1978 - 1984
参考文献
Nippon Shinyaku Co. Ltd.
Patent: US4241064 A1, 1980 ;
反应条件
1: 20 mg / diethyl ether / 10 h / Ambient temperature 2: 250 mg / KMnO4 / acetone 3: 280 mg / LiAlH4 / tetrahydrofuran / 5 h / Ambient temperature View Scheme
参考文献
Ohmoto, Taichi; Koike, Kazuo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3579 - 3583
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 5 h; Ambient temperature;
参考文献
Ohmoto, Taichi; Koike, Kazuo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3579 - 3583
反应条件
1: 520 mg / 5 percent H2SO4 / 2 h / Heating 2: 280 mg / LiAlH4 / tetrahydrofuran / 5 h / Ambient temperature View Scheme
参考文献
Ohmoto, Taichi; Koike, Kazuo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3579 - 3583
反应条件
1: 250 mg / KMnO4 / acetone 2: 280 mg / LiAlH4 / tetrahydrofuran / 5 h / Ambient temperature View Scheme
参考文献
Ohmoto, Taichi; Koike, Kazuo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3579 - 3583
反应条件
1: 69 percent / aq. H2SO4 / 6 h 2: 75 percent / H2O; methanol / 5 h / 25 °C / +0.7V/56mA; anode: graphite felt, cathode: Pt, electrolyte: KH2PO4/K2HPO4 View Scheme
参考文献
Bobbitt, James M.; Willis, John P.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1978 - 1984
反应条件
1: 96 percent / aq. HCl / 6 h / Heating 2: 35 percent / H2O; methanol / 5 h / 25 °C / +1.0V/30mA; anode: graphite felt, cathode: Pt, electrolyte: KH2PO4/K2HPO4 View Scheme
参考文献
Bobbitt, James M.; Willis, John P.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1978 - 1984
