(2R,3R,5S,6S)-5,6-双(羟甲基)-2,3-二甲氧基-2,3-二甲基-1,4-二氧己环合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 0.5 h;
参考文献
Barlow, Jaqueline S.; Dixon, Darren J.; Foster, Alison C.; Ley, Steven V.; Reynolds, Dominic J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1627 - 1629
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: With methanol in tetrahydrofuran; hexane T=-78°C; 0.25 h; 3: With sodium tetrahydroborate in methanol T=0 - 20°C;
参考文献
Maycock, Christopher D.; Rita Ventura
Tetrahedron Asymmetry, 2012 , vol. 23, # 17 p. 1262 - 1271
反应条件
1: p-toluenesulfonic acid / 4 h / 70 °C / 70 Torr 2: 95 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Berens, Ulrich; Leckel, Dieter; Oepen, Susanne C.
Journal of Organic Chemistry, 1995 , vol. 60, # 25 p. 8204 - 8208
