2-氯-1-(2,3,4-三羟基苯基)乙烷-1-酮合成路线 （共 10 条）
反应条件
boron trifluoride diethyl etherate T=65°C; Friedel-Crafts reaction; 3 h;
参考文献
Venkateswarlu, Somepalli; Panchagnula, Gopala K.; Subbaraju, Gottumukkala V.
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 10 p. 2183 - 2185
反应条件
AlCl3, aluminium chloride in carbon disulfide T=0°C; Friedel Crafts acylation; 12.25 h; Reflux;
参考文献
Gupta, Anjali; Priya, Nivedita; Jalal, Sarah; Singh, Prabhjot; Chand, Karam; Raj, Hanumantharao G.; Parmar, Virinder S.; DePass, Anthony L.; Sharma, Sunil K.
Biochimie, 2010 , vol. 92, # 9 p. 1180 - 1185
反应条件
aluminium trichloride T=100°C;
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1928 , vol. <2> 118, p. 316
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 121, p. 256
反应条件
1: 135 °C 2: aluminium chloride / 100 °C View Scheme
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1928 , vol. <2> 118, p. 316
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 121, p. 256
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride Erhitzen des Reaktionsprodukts mit Wasser;
参考文献
Yamashita
Sci. Rep. Tohoku Univ., Ser. 1: Phys., Chem., Astron., 1935 , vol. # 24, p. 192,193
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1928 , vol. <2> 118, p. 316
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 121, p. 256
参考文献
Bruhns
Chemische Berichte, 1901 , vol. 34, p. 98
反应条件
1: sodium acetate; ethanol
2: pyridine
3: palladium/charcoal; acetic acid / 65 °C / Hydrogenation
4: aqueous sodium carbonate
View Scheme
参考文献
Davies et al.
Journal of the Chemical Society, 1950 , p. 3206,3212
反应条件
1: 85 percent / sodium acetate / ethanol / 6 h / Heating
2: acetic anhydride / 2 h / 90 °C
View Scheme
参考文献
Venkateswarlu, Somepalli; Panchagnula, Gopala K.; Subbaraju, Gottumukkala V.
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 10 p. 2183 - 2185
反应条件
sodium acetate in ethanol
6 h; Heating;
参考文献
Venkateswarlu, Somepalli; Panchagnula, Gopala K.; Subbaraju, Gottumukkala V.
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 10 p. 2183 - 2185
