1-(对甲氧基苯基)2-硝基丙烯合成路线 （共 27 条）
参考文献
Wallach; Mueller,H.
Justus Liebigs Annalen der Chemie, 1904 , vol. 332, p. 319
反应条件
hydrogenchloride; iron(II) chloride in ethanol
参考文献
Ferreira,A.B.B.; Salisbury,K.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1978 , p. 995 - 1001
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux 2: Candida antartica lipase B; triethylamine / 35 °C / Inert atmosphere; Enzymatic reaction 3: water; potassium hydroxide / Reflux View Scheme
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux 2: hydrogen bromide / water / 3 h / Reflux View Scheme
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
hydrogenchloride; iron(III) chloride; iron
参考文献
Dumpis, M. A.; Kudryashova, N. I.; Veresova, M. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 7.2 p. 1332 - 1337
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 7 p. 1477 - 1482
反应条件
sulfuric acid; toluene-4-sulfonic acid in methanol T=0 - 5°C; ceramic diaphragm, carbon-rod anode, platinum cathode, 4.5 F/mol, 0.1A, cathode potential -1.45 to -1.65V vs. SCE;
参考文献
Journal of Organic Chemistry, , vol. 48, # 12 p. 2103 - 2105
反应条件
anhydrous iron chloride in ethylene glycol T=100°C; 8 h;
参考文献
Li, Liang; Zhao, Mi-Na; Ren, Zhi-Hui; Li, Jianli; Guan, Zheng-Hui
Synthesis, 2012 , vol. 44, # 4 p. 532 - 540
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux 2: hydrogen bromide / water / 3 h / Reflux 3: Candida antartica lipase B; triethylamine / 96 h / 35 °C / Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
copper(ll) bromide in ethanol T=110°C; 4 h; Green chemistry;
参考文献
Chen, Yongxin; Li, Kangning; Zhao, Mingming; Li, Yuanjiao; Chen, Baohua
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1627 - 1630
反应条件
formic acid; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; triethylamine; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in ethyl acetate
T=28°C; 5 h; chemoselective reaction;
参考文献
Xiang, Jing; Sun, Er-Xiao; Lian, Chun-Xia; Yuan, Wei-Cheng; Zhu, Jin; Wang, Qiwei; Deng, Jingen
Tetrahedron, 2012 , vol. 68, # 24 p. 4609 - 4620
