1-(对甲氧基苯基)2-硝基丙烯合成路线 （共 27 条）
反应条件
1: sodium methoxide / benzene / 1 h / 0 °C
2: LiAlH4 / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Osorio-Olivares, Mauricio; Rezende, Marcos Caroli; Sepulveda-Boza, Silvia; Cassels, Bruce K.; Fierro, Angelica
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 15 p. 4055 - 4066
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Redelfs, Elke; Ruhr, Maria
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1853 - 1859
反应条件
lithium aluminium tetrahydride in diethyl ether
3 h; Inert atmosphereReflux;
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
sulfuric acid; toluene-4-sulfonic acid in methanol
T=0 - 5°C; ceramic diaphragm, carbon-rod anode, platinum cathode, 4.5 F/mol, 0.1A, cathode potential -1.45 to -1.65V vs. SCE;
参考文献
Shono, Tatsuya; Hamaguchi, Hiroshi; Mikami, Hiroshi; Nogusa, Hideo; Kashimura, Shigenori
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2103 - 2105
反应条件
sulfuric acid in water; isopropyl alcohol
T=10 - 15°C; electrolysis; Yield given;
参考文献
Wessling, Michael; Schaefer, Hans J.
Chemische Berichte, 1991 , vol. 124, # 10 p. 2303 - 2306
反应条件
sulfuric acid in water; isopropyl alcohol
T=10 - 15°C; electrolysis; Yields of byproduct given;
参考文献
Wessling, Michael; Schaefer, Hans J.
Chemische Berichte, 1991 , vol. 124, # 10 p. 2303 - 2306
反应条件
acetic acid; zinc
high-melting form;
参考文献
Toennies
Chemische Berichte, 1887 , vol. 20, p. 2986
Full Text Show Details
Wallach; Mueller,H.
Justus Liebigs Annalen der Chemie, 1904 , vol. 332, p. 314,322
