17356-08-0合成路线 （共 1741 条）
反应条件
in dimethyl sulfoxide
T=155°C; 5 h; Microwave irradiationSealed vial; Product distribution / selectivity;
参考文献
The University of Houston
Patent: US2012/283436 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
in methanol
0.5 h; Ambient temperature; Mechanism;
参考文献
Naddaka, V. I.; Avanesyan, K. V.; Cherkinskaya, M. L.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2245 - 2250
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2489 - 2494
反应条件
in neat (no solvent)
passing Cl2 into thiourea about longer time;;
参考文献
Gmelin Handbook: Cl: SVol.B2, 75, page 483 - 485
反应条件
PEG-400 in water
0.0333333 h; microwave irradiation;
参考文献
Li, Zheng; Wang, Zhi-Yuan; Zhao, Yan-Long; Xing, Yu-Lin; Zhu, Wei
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 12 p. 2745 - 2750
反应条件
hydrogen bromide
Erwaermen des Reaktionsgemisches mit wss.Natronlauge;
参考文献
Kabatschnik et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2182,2189;engl.Ausg.S.2149,2155
反应条件
anschliessend mit wss.Natronlauge;
参考文献
Feher; Vogelbruch
Chemische Berichte, 1958 , vol. 91, p. 996,1001
反应条件
anschliessend mit wss.Natronlauge;
参考文献
Feher; Vogelbruch
Chemische Berichte, 1958 , vol. 91, p. 996,1001
反应条件
hydrogenchloride in ethanol
T=20°C; 24 h;
参考文献
AMBIT BIOSCIENCES CORPORATION
Patent: WO2009/38757 A2, 2009 ;
Location in patent: Page/Page column 84 ;
反应条件
hydrogen bromide
Kochen der Isothiuroniumsalz-Loesung mit verd.NaOH unter Stickstoff;
参考文献
Frank; Smith
Journal of the American Chemical Society, 1946 , vol. 68, p. 2104
反应条件
CuCl2·2H2O in ethanol; chloroform
T=80°C; 8 h;
参考文献
Khairullina; Geniyatova; Ibragimov; Dzhemilev
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 6 p. 904 - 908
Zh. Org. Khim., 2013 , vol. 49, # 6 p. 918 - 922,5
