17356-08-0合成路线 （共 1741 条）
反应条件
hydrogen bromide durch Kochen der entstandenen Isothiuroniumsalz-Loesung mit verd. NaOH unter Stickstoff;
参考文献
Frank; Smith
Journal of the American Chemical Society, 1946 , vol. 68, p. 2104
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Backer; Dijkstra
Recueil des Travaux Chimiques des Pays-Bas, 1932 , vol. 51, p. 290
反应条件
1: ethane-1,2-dial With phosphorous pentoxide; water T=20°C; 0.0833333 h; 2: thiourea T=20°C; 0.166667 h;
参考文献
Tetrahedron Letters, , vol. 52, # 14 p. 1713 - 1717
反应条件
in isopropyl alcohol T=85°C; 16 h; Heating / reflux;
参考文献
EP1908748 A1, ;
Page/Page column 8 ;
参考文献
Molecules, , vol. 11, # 10 p. 739 - 750
参考文献
Journal of the Chemical Society, , p. 559
反应条件
sodium methylate in methanol T=65°C; 8 h;
参考文献
Medicinal Chemistry Research, , vol. 22, # 9 p. 4075 - 4086
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 35, p. 456
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 49, p. 38
反应条件
in dimethylsulfoxide-d6 T=22 - 28°C; pH = 1-2; Mechanism;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 2087 - 2093
反应条件
1: methylglyoxylate methanol hemiacetal; N,N-dimethyl-formamide dimethyl acetal T=80 - 109°C; 18 h; Heating / reflux; 2: thiourea in methanol T=20°C; 0.25 h; 3: methyl iodide With sodium methylate more than 3 stages;
参考文献
Laufersweiler, Matthew John; Crago Clark, Cynthia Monesa; Clark, Michael Philip; Djung, Jane Far-Jine; De, Biswanath; Natchus, Michael George
Patent: US2003/225082 A1, 2003 ;
Location in patent: Page 8-9 ;
参考文献
English et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 453,457
