17356-08-0合成路线 （共 1741 条）
反应条件
(i) PhSO2Cl, (ii) /BRN= 605327/; Multistep reaction;
参考文献
Miryan,N.I. et al.
Pharmaceutical Chemistry Journal, 1973 , vol. 7, # 8 p. 489 - 491
Khimiko-Farmatsevticheskii Zhurnal, 1973 , vol. 7, # 8 p. 17 - 20
参考文献
Eastman Kodak Co.
Patent: US2423709 , 1945 ;
Full Text Show Details
Knott
Journal of the Chemical Society, 1945 , p. 455,457
反应条件
hydrogenchloride
T=130°C;
参考文献
Werner
Journal of the Chemical Society, 1916 , vol. 109, p. 1128
参考文献
Kohmann
Journal of the American Chemical Society, 1915 , vol. 37, p. 2132
参考文献
Dixon; Taylor
Journal of the Chemical Society, 1920 , vol. 117, p. 727
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Werner
Journal of the Chemical Society, 1916 , vol. 109, p. 1128
Full Text Show Details
Hugershoff
Chemische Berichte, 1925 , vol. 58, p. 2482
Full Text Show Details
Lecher; Siefken
Justus Liebigs Annalen der Chemie, 1927 , vol. 456, p. 199
反应条件
methanol
Erhitzen des Reaktionsprodukts mit wss.Natronlauge und anschliessend mit Jodmethan;
参考文献
Jurecek et al.
Chemicke Listy, 1954 , vol. 48, p. 542,545
Chem.Abstr., 1954 , p. 8129
参考文献
Miller et al.
Journal of the American Chemical Society, 1940 , vol. 62, p. 2099,2101
反应条件
in neat (no solvent)
byproducts: water, ammonia; mixt. (molar ratio Sn-compd.:thiourea=2:1) heating up to 250°C in 1 h (gradual evacuation from 50 to 1.33 hPa); distn. of Bu3SnNCS after no water and ammonia came off; (Bu3Sn)2S isolation from residue;
参考文献
Gordetsov, A. S.; Latyaeva, V. N.; Bogdarin, Yu. A.; Boyarinov, G. A.; Dergunov, Yu. I.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 770 - 774
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 885 - 890
反应条件
in water
3 h; Heating;
参考文献
Monge; Martinez-Merino; Cenarruzabeitia; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 1 p. 61 - 66
反应条件
bromine; methyloxirane in acetonitrile
T=10 - 20°C;
参考文献
Soroka, Miroslaw; Goldeman, Waldemar
Tetrahedron, 2005 , vol. 61, # 17 p. 4233 - 4235
