3-(4-羟基苯基)丙酸合成路线 (共 21 条)
反应条件
boron tribromide in dichloromethane T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 18 p. 2704 - 2707
反应条件
1: Bu4NCl; NaHCO3 / Pd(OAc)2 / dimethylformamide / 40 °C 2: Mg / methanol / 20 °C 3: BBr3 / CH2Cl2 / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 18 p. 2704 - 2707
反应条件
1: (4-hydroxyphenyl)-acetic acid With indium tribromide; 1,1,3,3-tetramethyldisiloxane; iodine in chloroform T=60°C; Inert atmosphere; 2: trimethylsilyl cyanide With tetrabutyl ammonium fluoride in tetrahydrofuran; chloroform T=60°C; 5 h; Inert atmosphere; Reagent/catalyst; chemoselective reaction;
参考文献
Moriya, Toshimitsu; Shoji, Kohei; Yoneda, Shinichiro; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Synthesis (Germany), 2013 , vol. 45, # 23 p. 3233 - 3238
反应条件
1: Mg / methanol / 20 °C 2: BBr3 / CH2Cl2 / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 18 p. 2704 - 2707
反应条件
hydrogenchloride; aluminium trichloride 2 h; Heating;
参考文献
Dong, Chang-Zhi; Ahamada-Himidi, Azali; Plocki, Stephanie; Aoun, Darina; Touaibia, Mohamed; Meddad-Bel Habich, Nadia; Huet, Jack; Redeuilh, Catherine; Ombetta, Jean-Edouard; Godfroid, Jean-Jacques; Massicot, France; Heymans, Francoise
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 1989 - 2007
反应条件
trifluorormethanesulfonic acid; [NBu4][ReO4] in 1,2-dichloro-ethane Heating;
参考文献
Kusama, Hiroyuki; Uchiyama, Katsuya; Yamashita, Yuko; Narasaka, Koichi
Chemistry Letters, 1995 , # 8 p. 715 - 716
反应条件
in water Irradiation (UV/VIS); photolyses in room temp. aq. soln. at 313 or 254 nm;
参考文献
Inorganic Chemistry, , vol. 20, p. 1764 - 1767
参考文献
Chemische Berichte, , vol. 50, p. 618
Chem. Zentralbl., , vol. 87, # II p. 1025
反应条件
sulfuric acid Diazotization;
参考文献
Chemische Berichte, , vol. 61, p. 2492
反应条件
1: tin; hydrochloric acid; alcohol / 50 °C 2: diluted sulfuric acid / Diazotization View Scheme
参考文献
Chemische Berichte, , vol. 61, p. 2492