正辛基 2-乙酰氨基-3,4,6-O-三乙酰基-2-脱氧-beta-D-吡喃葡萄糖苷合成路线 （共 8 条）
反应条件
silica-gel-supported sulfuric acid in 1,2-dichloro-ethane T=110°C; 0.25 h; Microwave irradiation; stereoselective reaction;
参考文献
Mandai, Santanu; Sharma, Nayan; Mukhopadhyay, Balaram
Synlett, 2009 , # 19 p. 3111 - 3114
反应条件
3 A molecular sieve; mercury(II) iodide in 1,2-dichloro-ethane T=90 - 95°C; 0.5 h; Yields of byproduct given;
参考文献
Zemlyakov; Kur'yanov; Sidorova; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 8 p. 551 - 558
反应条件
N-iodo-succinimide; copper(II) bis(trifluoromethanesulfonate) in dichloromethane 4.5 h; Inert atmosphereReflux;
参考文献
Krag, Jonas; Christiansen, Mira S.; Petersen, Jette G.; Jensen, Henrik H.
Carbohydrate Research, 2010 , vol. 345, # 7 p. 872 - 879
反应条件
4 A molecular sieve; iodine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile 12 h; Ambient temperature;
参考文献
Kartha, K.P. Ravindranathan; Aloui, Mahmoud; Field, Robert A.
Tetrahedron Letters, 1996 , vol. 37, # 48 p. 8807 - 8810
反应条件
anhydrous potassium sulfate; iron(III) chloride in dichloromethane 16 h; Ambient temperature;
参考文献
Ogawa, Seiichiro; Matsunaga, Naoki; Li, Hong; Palcic, Monica M.
European Journal of Organic Chemistry, 1999 , # 3 p. 631 - 642
反应条件
N-iodo-succinimide; scandium tris(trifluoromethanesulfonate) in dichloromethane 3 h; Inert atmosphereReflux;
参考文献
Krag, Jonas; Christiansen, Mira S.; Petersen, Jette G.; Jensen, Henrik H.
Carbohydrate Research, 2010 , vol. 345, # 7 p. 872 - 879
反应条件
1: NaOMe / pyridine / Ambient temperature 2: 44 percent / potassium sulfate, ferric chloride / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 631 - 642
反应条件
sodium methylate in methanol Zemplen deacetylation;
参考文献
Zemlyakov; Tsikalov; Kalyuzhin; Kur'yanov; Chirva
Russian Journal of Bioorganic Chemistry, 2003 , vol. 29, # 3 p. 286 - 292
