N-苄基-4-甲氧基苯胺合成路线 (共 83 条)
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in toluene T=70°C; 24 h; Inert atmosphere;
参考文献
Li, Jianhui; Wang, Zhouyu; Jiang, Zhenju; Jiang, Shengqian; Xiong, Lilin
Asian Journal of Chemistry, 2011 , vol. 23, # 9 p. 4101 - 4103
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in neat (no solvent) T=150°C; 0.25 h; Molecular sieve; TemperatureTime;
参考文献
Nguyen, Quynh Pham Bao; Kim, Taek Hyeon
Tetrahedron, 2013 , vol. 69, # 24 p. 4938 - 4943
反应条件
potassium phosphate; copper(l) iodide; CVT-2537 in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Zhang, Yu; Yang, Xinye; Yao, Qizheng; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 12 p. 3056 - 3059
反应条件
cyclohexyl BrettPhos; BrettPhos palladium(II) phenethylamine chloride; sodium t-butanolate in anhydrous butyl ether T=85°C; 1 h; Inert atmosphere;
参考文献
Fors, Brett P.; Watson, Donald A.; Biscoe, Mark R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13552 - 13554
反应条件
tetra(n-butyl)ammonium hydroxide; copper(l) chloride in water T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Hua-Jian; Zheng, Fa-Yin; Liang, Yu-Feng; Cai, Zhen-Ya; Feng, Yi-Si; Che, Da-Qing
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 669 - 671
反应条件
5 Au/Fe2O3; hydrogen in toluene T=120°C; P=15001.5 Torr; 6 h; Autoclave;
参考文献
Yamane, Yoshihiro; Liu, Xiaohao; Hamasaki, Akiyuki; Ishida, Tamao; Haruta, Masatake; Yokoyama, Takushi; Tokunaga, Makoto
Organic Letters, 2009 , vol. 11, # 22 p. 5162 - 5165
反应条件
Cp*Ir(Pro)Cl in toluene T=95°C; 24 h; Inert atmosphereSealed tube;
参考文献
Wetzel, Alexander; Woeckel, Simone; Schelwies, Mathias; Brinks, Marion K.; Rominger, Frank; Hofmann, Peter; Limbach, Michael
Organic Letters, 2013 , vol. 15, # 2 p. 266 - 269
反应条件
sodium t-butanolate; Pd(dba)2 in toluene
参考文献
Yale University
Patent: US6562989 B2, 2003 ;
反应条件
potassium phosphate; copper monoiodide in ethylene glycol
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 12, # 12 p. 2606 - 2609,2516 - 2518
Chemische Berichte, , vol. 40, p. 1010