N-苄基-4-甲氧基苯胺合成路线 （共 83 条）
反应条件
1: 1.) butyllithium / 1.) THF, 0-20 deg C, 12 h, 2.) 0-20 deg C, 5 h 2: 99 percent / tetrabutylammonium dihydrogentrifluoride, NBS / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Kanie, Kiyoshi; Mizuno, Katsuya; Kuroboshi, Manabu; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 8 p. 1973 - 1991
反应条件
W4 Raney nickel in anhydrous xylene 32 h; Reflux;
参考文献
Mehta, Astha; Thaker; Londhe; Nandan, Santosh R.
Applied Catalysis A: General, 2014 , vol. 478, p. 241 - 251
反应条件
ammonium formate; zinc in ethylene glycol 0.0466667 h; microwave irradiation;
参考文献
Babu, S.N. Narendra; Srinivasa; Santhosh; Gowda, D. Channe
Journal of Chemical Research, 2004 , # 1 p. 66 - 67
反应条件
oxygen; Titanium(IV) oxide in acetonitrile P=760.051 Torr; 8 h; UV-irradiation;
参考文献
Lang, Xianjun; Ma, Wanhong; Zhao, Yubao; Chen, Chuncheng; Ji, Hongwei; Zhao, Jincai
Chemistry - A European Journal, 2012 , vol. 18, # 9 p. 2624 - 2631
反应条件
trichloroisocyanuric acid; sulfuric acid in acetonitrile T=21°C; 16 h;
参考文献
Verkade, Jorge M.M.; van Hemert, Lieke J.C.; Quaedflieg, Peter J.L.M.; Alsters, Paul L.; van Delft, Floris L.; Rutjes, Floris P.J.T.
Tetrahedron Letters, 2006 , vol. 47, # 46 p. 8109 - 8113
反应条件
1.1: triethylamine / 1.5 h / 80 °C 1.2: 68 percent / ZnCl2 / ethanol / 4 h / 110 °C 2.1: 83 percent / Na; NH3 / tetrahydrofuran / 1.5 h / -33 °C View Scheme
参考文献
Trost, Barry M.; Quancard, Jean
Journal of the American Chemical Society, 2006 , vol. 128, # 19 p. 6314 - 6315
反应条件
1: benzene; potassium hydroxide
View Scheme
参考文献
Wedekind
Chemische Berichte, 1906 , vol. 39, p. 483
Chemische Berichte, 1899 , vol. 32, p. 522,3565
反应条件
1: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chlorobenzene
T=20°C; 0.166667 h; Inert atmosphere;
2: With phenyl-magnesium bromide in anhydrous butyl ether; chlorobenzene
T=0°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro; Li, Chao-Jun
Organic Letters, 2013 , vol. 15, # 14 p. 3650 - 3653
反应条件
oxygen; cobalt(II)salen in ethanol
T=60°C; 2 h;
参考文献
Nishinaga, Akira; Yamazaki, Shigekazu; Matsuura, Teruo
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4115 - 4118
反应条件
1: 81 percent / NaHCO3 / CH2Cl2; H2O / Ambient temperature
2: 67 percent / NaHCO3 / acetonitrile; H2O / Irradiation
View Scheme
参考文献
Hamada; Okuno; Ohmori; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 1 p. 128 - 136
