N-苄氧羰基甘氨酸-4-硝基苯酯合成路线 (共 36 条)
反应条件
sodium hydroxide; N-hexadecyl-N,N,N-trimethylammonium bromide in water; butan-1-ol T=25°C; rate constant of pseudofirst-order aminolysis in two phase system; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, p. 2306 - 2311
Zhurnal Organicheskoi Khimii, , vol. 23, # 12 p. 2612 - 2617
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water 40 h; Yield given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2592 - 2597
反应条件
water in chloroform T=25°C; phase-transfer catalysis (ammonium salts), buffer solution (pH 9), oth. org. solvents; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 8 p. 1583 - 1588
Zhurnal Organicheskoi Khimii, , vol. 23, # 8 p. 1775 - 1781
反应条件
triethylamine in water; acetonitrile
T=20°C; 1.66667 h;
参考文献
Gagnon, Paul; Huang, Xicai; Therrien, Eric; Keillor, Jeffrey W.
Tetrahedron Letters, 2002 , vol. 43, # 43 p. 7717 - 7719
参考文献
Sandrin,E.; Boissonnas,R.A.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1637 - 1669
参考文献
Kawasaki; Tsuji; Hirase; Miyano; Imoto; Iwamoto
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 584 - 589
反应条件
1-ethyl-piperidine in N,N-dimethyl-formamide
12 h; Ambient temperature; Yield given;
参考文献
Hauzer, Karel; Servitova, Linda; Barth, Tomislav; Jost, Karel
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 4 p. 1139 - 1148
反应条件
sodium hydroxide in 1,4-dioxane
48 h;
参考文献
Kuranova, I. L.; Churkina, S. I.; Os'mak, A. V.; Filonova, E. B.; Lyudmirova, V. L.; Noskova, O. V.
Chemistry of Natural Compounds, 1992 , vol. 28, # 3/4 p. 355 - 361
Khimiya Prirodnykh Soedinenii, 1992 , # 3,4 p. 406 - 413
反应条件
sodium hydroxide; N-hexadecyl-N,N,N-trimethylammonium bromide in water; butan-1-ol
T=25°C; rate constant of pseudofirst-order aminolysis in two phase system; Rate constant;
参考文献
Kosmynin, V. V.; Kaida, L. N.; Savelova, V. A.; Taran, N. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 2306 - 2311
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 12 p. 2612 - 2617
参考文献
DeTar,D.F. et al.
Journal of the American Chemical Society, 1966 , vol. 88, # 5 p. 1024 - 1030