N-苄氧羰基-1,3-二氨基丙烷盐酸盐合成路线 (共 6 条)
反应条件
triphenylphosphine in tetrahydrofuran; water T=20°C; 24 h;
参考文献
Lee, Jae Wook; Jun, Sung Im; Kim, Kimoon
Tetrahedron Letters, 2001 , vol. 42, # 14 p. 2709 - 2711
反应条件
sodium tetrahydroborate; nickel dichloride in methanol 0.5 h; Ambient temperature;
参考文献
Constantinou-Kokotou, Violetta; Kokotos, George
Organic Preparations and Procedures International, 1994 , vol. 26, # 5 p. 599 - 602
反应条件
1: Et3N / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT, 30 min 2: dimethylformamide / 3 h / 60 °C 3: 71 percent / NaBH4, NiCl2*6H2O / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 26, # 5 p. 599 - 602
反应条件
1: dimethylformamide / 3 h / 60 °C 2: 71 percent / NaBH4, NiCl2*6H2O / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 26, # 5 p. 599 - 602
反应条件
hydrogenchloride in acetic acid Yield given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 11 p. 1224 - 1227
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1540 - 1544
反应条件
hydrogen; palladium on activated charcoal in methanol 4 h; Yield given;
参考文献
Constantinou-Kokotou, Violetta; Kokotos, George
Organic Preparations and Procedures International, 1994 , vol. 26, # 5 p. 599 - 602