6-乙炔基-1,3,5-环庚三烯-1-羧酸合成路线 （共 3 条）
反应条件
potassium hydroxide in water; N,N-dimethyl-formamide
参考文献
Higuchi, Hiroyuki; Kiyoto, Seiken; Sakon, Chiaki; Hiraiwa, Naoki; Asano, Kaori; et al.
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 12 p. 3519 - 3538
反应条件
1: 1.) aluminium chloride / 1.) CH2Cl2, 10 min, reflux, 2.) CH2Cl2, 4 h, 40 deg C 2: 57 percent / phosphoryl chloride / dimethylformamide; benzene / 21 h / Ambient temperature 3: 3 percent / 15 M aq. KOH / dimethylformamide; H2O View Scheme
参考文献
Higuchi, Hiroyuki; Kiyoto, Seiken; Sakon, Chiaki; Hiraiwa, Naoki; Asano, Kaori; et al.
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 12 p. 3519 - 3538
反应条件
1: 57 percent / phosphoryl chloride / dimethylformamide; benzene / 21 h / Ambient temperature 2: 3 percent / 15 M aq. KOH / dimethylformamide; H2O View Scheme
参考文献
Higuchi, Hiroyuki; Kiyoto, Seiken; Sakon, Chiaki; Hiraiwa, Naoki; Asano, Kaori; et al.
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 12 p. 3519 - 3538
