5-三乙硅基-4-戊炔-1-醇合成路线 (共 2 条)
反应条件
1: 5-hydroxypentyne With n-butyllithium in tetrahydrofuran; toluene T=-68°C; 1 h; 2: triethylsilyl chloride in tetrahydrofuran; toluene T=-68 - 20°C; 20 h; 3: With hydrogenchloride in tetrahydrofuran; toluene T=20°C; 48 h;
参考文献
Wennekes, Tom; Van Den Berg, Richard J. B. H. N.; Donker, Wilma; Van Der Marel, Gijsbert A.; Strijland, Anneke; Aerts, Johannes M. F. G.; Overkleeft, Herman S.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1088 - 1097
参考文献
Brinkmann, Christine; Barrett, Anthony G. M.; Reid, Stephanie; Hill, Michael S.; Procopiou, Panayiotis A.
Organometallics, 2012 , vol. 31, # 20 p. 7287 - 7297,11