4,4,5,5-四甲基-2-(1-苯基乙基)-1,3,2-二噁硼烷合成路线 （共 44 条）
反应条件
sodium hydroxide; dihydrogen peroxide in diethyl ether; cyclohexane T=20°C; 1 h;
参考文献
Larouche-Gauthier, Robin; Fletcher, Catherine J.; Couto, Irantzu; Aggarwal, Varinder K.
Chemical Communications, 2011 , vol. 47, # 47 p. 12592 - 12594
反应条件
1: in tetrahydrofuran; hexane T=-78 - 20°C; Substitution; Homologation; 2: With sodium hydroxide; dihydrogen peroxide in methanol; diethyl ether T=20°C; Oxidation;
参考文献
Ren, Li; Crudden, Cathleen M.
Chemical Communications (Cambridge, United Kingdom), 2000 , # 8 p. 721 - 722
反应条件
styrene; tetrakis(triphenylphosphine) palladium(0); water; potassium carbonate; triphenylphosphine; silver(l) oxide in ethylene glycol dimethyl ether
T=85°C; Suzuki-Miyaura Coupling; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Glasspoole, Ben W.; Oderinde, Martins S.; Moore, Brandon D.; Antoft-Finch, Aurora; Crudden, Cathleen M.
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0347-OP, p. 1759 - 1763
反应条件
styrene; tetrakis(triphenylphosphine) palladium(0); water; potassium carbonate; triphenylphosphine; silver(l) oxide in ethylene glycol dimethyl ether
T=85°C; Suzuki-Miyaura Coupling; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Glasspoole, Ben W.; Oderinde, Martins S.; Moore, Brandon D.; Antoft-Finch, Aurora; Crudden, Cathleen M.
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0347-OP, p. 1759 - 1763
