5-溴-2-苯基苯并咪唑合成路线 （共 11 条）
反应条件
indium; acetic acid in ethyl acetate 1.5 h; RefluxInert atmosphere;
参考文献
Kim, Jaeho; Kim, Jihye; Lee, Hyunseung; Lee, Byung Min; Kim, Byeong Hyo
Tetrahedron, 2011 , vol. 67, # 41 p. 8027 - 8033
反应条件
PIDA; caesium carbonate in 2,2,2-trifluoroethanol T=0°C; 1.5 h;
参考文献
Huang, Jinbo; He, Yimiao; Wang, Yong; Zhu, Qiang
Chemistry - A European Journal, 2012 , vol. 18, # 44 p. 13964 - 13967
反应条件
air in 1,4-dioxane T=100°C; 6 h;
参考文献
Lin, Songnian; Yang, Lihu
Tetrahedron Letters, 2005 , vol. 46, # 25 p. 4315 - 4319
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Xiang, Shi-Kai; Tan, Wen; Zhang, Dong-Xue; Tian, Xian-Li; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7271 - 7275
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=120°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Xiang, Shi-Kai; Tan, Wen; Zhang, Dong-Xue; Tian, Xian-Li; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7271 - 7275
反应条件
potassium carbonate in water T=100°C; 30 h; Schlenk techniqueGreen chemistry;
参考文献
Chen, Chunxia; Chen, Chen; Li, Bin; Tao, Jingwei; Peng, Jinsong
Molecules, 2012 , vol. 17, # 11 p. 12506 - 12520
反应条件
peracetic acid; iodobenzene T=50°C; 1.5 h;
参考文献
He, Yimiao; Huang, Jinbo; Liang, Dongdong; Liu, Lanying; Zhu, Qiang
Chemical Communications, 2013 , vol. 49, # 66 p. 7352 - 7354
反应条件
1: |Inert atmosphere 2: PIDA; caesium carbonate / 2,2,2-trifluoroethanol / 1.5 h / 0 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 44 p. 13964 - 13967
反应条件
1: Bromieren 2: tin; hydrochloric acid View Scheme
参考文献
Chemische Berichte, , vol. 10, p. 1710
反应条件
1: AlCl3, aluminium chloride / 1 h / 130 °C / |Inert atmosphere; |Sealed tube 2: iodobenzene; peracetic acid / 1.5 h / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 66 p. 7352 - 7354
