(二异丙基氨基)三甲基硅烷合成路线 （共 10 条）
反应条件
chloro-trimethyl-silane; iodine; magnesium
参考文献
Temple University-Of The Commonwealth System of Higher Education
Patent: US5863905 A1, 1999 ;
反应条件
1: diisopropylamine With n-butyllithium in diethyl ether; hexane T=-20 - 20°C; Inert atmosphere; 2: chloro-trimethyl-silane in diethyl ether; hexane T=-78 - 20°C; 18.5 h; Inert atmosphere;
参考文献
Schulz, Felix; Sumerin, Victor; Leskelae, Markku; Repo, Timo; Rieger, Bernhard
Dalton Transactions, 2010 , vol. 39, # 8 p. 1920 - 1922
参考文献
Lipshutz, Bruce H.; Wood, Michael R.; Lindsley, Craig W.
Tetrahedron Letters, 1995 , vol. 36, # 25 p. 4385 - 4388
参考文献
Gibson,J.A. et al.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 3203 - 3210
反应条件
multistep; reaction of aldoxime anions; also with D2O; further agents; neutralization with NH4Cl or HCl; Product distributionMechanism;
参考文献
Hassner, Alfred; Naeumann, Fritz
Chemische Berichte, 1988 , vol. 121, p. 1823 - 1826
参考文献
Seppelt,K.; Sundermeyer,W.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1969 , vol. 24, p. 774
反应条件
1: diethyl ether / 20 h / Ambient temperature 2: tetrahydrofuran / according to ref 3) with modifications View Scheme
参考文献
Sinha, N. D.; Biernat, J.; Koester, H.
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5843 - 5846
反应条件
1: diethyl ether / 20 h / Ambient temperature 2: tetrahydrofuran / according to ref 3) with modifications View Scheme
参考文献
Sinha, N. D.; Biernat, J.; Koester, H.
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5843 - 5846
反应条件
1: diethyl ether / 20 h / Ambient temperature 2: tetrahydrofuran / according to ref 3) with modifications View Scheme
参考文献
Sinha, N. D.; Biernat, J.; Koester, H.
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5843 - 5846
反应条件
thionyl chloride in diethyl ether
T=-78°C;
参考文献
Neidlein, Richard; Walser, Peter
Chemische Berichte, 1982 , vol. 115, # 7 p. 2428 - 2436
