1,1,1-三甲基-N,N-二苯基-硅烷胺合成路线 （共 18 条）
反应条件
1: diphenylamine With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=20°C; 18 h;
参考文献
Smith, Catherine J.; Tsang, Melanie W.S.; Holmes, Andrew B.; Danheiser, Rick L.; Tester, Jefferson W.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3767 - 3781
反应条件
(K-18-crown-6 ether) cyanide in tetrahydrofuran 2 h;
参考文献
Vyazankina, O. A.; Gostevskii, B. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1985 , vol. 292, p. 145 - 150
反应条件
18-crown-6 ether; potassium carbonate T=110°C; 3 h;
参考文献
Galan, Adam A.; Lee, Thomas V.; Chapleo, Christopher B.
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 4995 - 4998
反应条件
in tetrahydrofuran Ambient temperature;
参考文献
Nagy, Attila; Green, Jennifer C.; Szepes, Laszlo; Zanathy, Laszlo
Journal of Organometallic Chemistry, 1991 , vol. 419, # 1 p. 27 - 42
参考文献
Gemuend, Birgit; Noeth, Heinrich; Sachdev, Hermann; Schmidt, Martin
Chemische Berichte, 1996 , vol. 129, # 11 p. 1335 - 1344
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 0.5 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 1 h; Inert atmosphere;
参考文献
Chemistry Letters, , vol. 43, # 4 p. 438 - 440
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 0.5 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 4 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 0.5 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
