4-羟基-3,3,5,5-四甲基环己酮合成路线 （共 3 条）
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.5 h;
参考文献
Keana, John F. W.; Seyedrezai, Seyed E.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 347 - 352
反应条件
1: 12percent HCl, SiO2 (60-200 mesh) / CH2Cl2 / 1 h / 25 °C 2: 31 percent / NaBH4 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Keana, John F. W.; Seyedrezai, Seyed E.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 347 - 352
反应条件
(i) NaH, toluene, (ii) LiAlH4, Et2O, (iii) aq. AcOH; Multistep reaction;
参考文献
Green,M.M.; Djerassi,C.
Journal of the American Chemical Society, 1967 , vol. 89, p. 5190 - 5198
