1-苯基-3-丁炔-1-醇合成路线 （共 77 条）
反应条件
1,3-dimethyl-imidazolidin-2-one; bis(acetylacetonate)nickel(II); InI; triphenylphosphine in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Hirashita, Tsunehisa; Suzuki, Yuuki; Tsuji, Hiromitsu; Sato, Yoshiki; Naito, Kojiro; Araki, Shuki
European Journal of Organic Chemistry, 2012 , # 29 p. 5668 - 5672,5
Title/Abstract Full Text Show Details
Hirashita, Tsunehisa; Suzuki, Yuuki; Tsuji, Hiromitsu; Sato, Yoshiki; Naito, Kojiro; Araki, Shuki
European Journal of Organic Chemistry, 2012 , # 29 p. 5668 - 5672
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C;
参考文献
Yanagisawa; Habaue; Yamamoto
Tetrahedron, 1992 , vol. 48, # 11 p. 1969 - 1980
反应条件
1: diethyl prop-2-yn-1-yl phosphate With Bu5CrLi2 in tetrahydrofuran
T=-78°C; 0.5 h;
2: benzaldehyde in tetrahydrofuran
T=-78°C; 2 h; Further stages.;
参考文献
Hojo; Sakuragi; Okabe; Hosomi
Chemical Communications, 2001 , # 4 p. 357 - 358
反应条件
in diethyl ether; toluene
T=-78 - 20°C; 1 h;
参考文献
Tummatorn, Jumreang; Dudley, Gregory B.
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5050 - 5051
反应条件
n-butyllithium in diethyl ether
T=-20 - 20°C; 1 h;
参考文献
Cabezas, Jorge A.; Alvarez, Leonardo X.
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 3935 - 3938
反应条件
trifluoroacetic acid in methanol
T=25°C; 24 h;
参考文献
McCluskey; Muderawan; Muntari; Young
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7811 - 7817
反应条件
1: With Cl(3)HO4 in dichloromethane
T=-20°C; 6.5 h;
2: With tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Niimi, Lui; Hiraoka, Shuichi; Yokozawa, Tsutomu
Tetrahedron, 2002 , vol. 58, # 2 p. 245 - 252
反应条件
in tetrahydrofuran; diethyl ether
T=20°C; 1 h;
参考文献
Maddess, Matthew L.; Lautens, Mark
Organic Letters, 2005 , vol. 7, # 16 p. 3557 - 3560
反应条件
sodium hydroxide in N,N-dimethyl-formamide
参考文献
Sumitomo Chemical Company, Limited
Patent: US5258529 A1, 1993 ;
反应条件
ytterbium(III) triflate in tetrahydrofuran
T=20°C; Addition; 96 h;
参考文献
Shim, Jae-Goo
Journal of Organometallic Chemistry, 1999 , vol. 588, # 1 p. 20 - 21
