1-苯基-3-丁炔-1-醇合成路线 （共 77 条）
反应条件
ammonia in diethyl ether
参考文献
Marvell,E.N. et al.
Tetrahedron, 1973 , vol. 29, p. 3797 - 3806
反应条件
stannous iodide; water; tetra-(n-butyl)ammonium iodide in various solvent(s)
T=25°C; 47 h; Yields of byproduct given;
参考文献
Masuyama, Yoshiro; Ito, Akihiro; Fukuzawa, Mamiko; Terada, Kohji; Kurusu, Yasuhiko
Chemical Communications, 1998 , # 18 p. 2025 - 2026
反应条件
ammonium chloride; zinc in water
1 h;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.; Da Costa, Rosenildo C.; Silva, Lilia O.S.
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3655 - 3658
反应条件
in tetrahydrofuran
T=0°C; 0.5 h; Title compound not separated from byproducts.;
参考文献
Kribber, Thomas; Labonne, Aurelie; Hintermann, Lukas
Synthesis, 2007 , # 18 p. 2809 - 2818
反应条件
in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Kribber, Thomas; Labonne, Aurelie; Hintermann, Lukas
Synthesis, 2007 , # 18 p. 2809 - 2818
反应条件
1: zinc; bromobenzene / tetrahydrofuran / |Reflux
2: tetrahydrofuran / 20 °C
View Scheme
参考文献
Wu, Chao; Huang, Wangyong; He, Weimin; Xiang, Jiannan
Chemistry Letters, 2013 , vol. 42, # 10 p. 1233 - 1234
反应条件
tin; hydrogen bromide in tetrahydrofuran
2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Wu, Shihui; Huang, Bangzhou; Gao, Xiang
Synthetic Communications, 1990 , vol. 20, # 9 p. 1279 - 1286
反应条件
T=-40 - 20°C; Inert atmosphere;
参考文献
Cheng, Xin; Jiang, Xuefeng; Yu, Yihua; Ma, Shengming
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8960 - 8965
反应条件
tetrabutyl ammonium fluoride
1.) THF, 0 deg C, 2.) THF; Multistep reaction. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Habaue, Shigeki; Yamamoto, Hisashi
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5198 - 5200
反应条件
sodium hydroxide; dihydrogen peroxide
1) Et2O, 25 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Khire, Uday R.; Racherla, Uday S.
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 15 - 18
