1,4-二甲基-4-乙烯基环己烯合成路线 (共 12 条)
反应条件
alpha-acetoxyacrylonitrile Irradiation;
参考文献
Hammond,G.S. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 3297 - 3303
反应条件
diethylaluminium chloride; titanium tetrachloride in benzene T=60°C; 6 h; in a sealed ampoule; Yield given;
参考文献
Mach, K.; Antropiusova, H.; Petrusova, L.; Turecek, F.; Hanus, V.; et al.
Journal of Organometallic Chemistry, 1985 , vol. 289, p. 331 - 340
参考文献
Hammond,G.S. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 3297 - 3303
反应条件
triphenyl phosphite; bis(acetylacetonate)nickel(II); 1,2-dimethylenecyclobutane; triethylaluminum in toluene T=100°C; 4 h; Further byproducts given;
参考文献
Dzhemilev, U.M.; Khusnutdinov, R.I.; Shchadneva, N.A.; Khalilov, L.M.; Tolstikov, G.A.; Nefedov, O.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 10 p. 2094 - 2099
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 10 p. 2294 - 2299
反应条件
palladium in tetrahydrofuran T=80°C; Yield given. Yields of byproduct given;
参考文献
Zenkevich
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 10 p. 1403 - 1409
反应条件
bis(acetylacetonate)nickel(II); tris(hexafluoroisopropyl) phosphite; triethylaluminum in tetrahydrofuran; 2,2,4-trimethylpentane 0.7 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Leeuwen, P. W. N. M. van; Roobeek, C. F.
Tetrahedron, 1981 , vol. 37, p. 1973 - 1984
反应条件
bis(acetylacetonate)nickel(II); tris(hexafluoroisopropyl) phosphite; triethylaluminum in tetrahydrofuran; 2,2,4-trimethylpentane 0.7 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Leeuwen, P. W. N. M. van; Roobeek, C. F.
Tetrahedron, 1981 , vol. 37, p. 1973 - 1984
反应条件
diethylaluminium chloride; Ti(IV)-komplexe in benzene dimerisierung aktivitaet des Ti(IV)-komplexes; Product distribution;
参考文献
Kauffmann, Thomas; Ennwn, Johann; Berghus, Karlheinz
Tetrahedron Letters, 1984 , vol. 25, # 19 p. 1971 - 1974
反应条件
bis(1-hydroxy-5-bromophenyl)sulphide; titanium tetrachloride in pentane T=120°C; 20 h; var. temp., var. reagent rates; Product distribution;
参考文献
Dieck, Heindirk tom; Mueller, Hartmut
Journal of Organometallic Chemistry, 1981 , vol. 221, # 1 p. C7 - C10
反应条件
bis(1,5-cyclooctadiene)nickel (0); (D)EPHOSNH T=40°C; 19 h; Product distribution;
参考文献
Denis; Jean; Croizy; Mortreux; Petit
Journal of the American Chemical Society, 1990 , vol. 112, # 3 p. 1292 - 1294