1,4-二甲基-4-乙烯基环己烯合成路线 (共 12 条)
反应条件
bis(acetylacetonate)nickel(II); [(CF3)2CHO]3P; triethylaluminum in tetrahydrofuran; 2,2,4-trimethylpentane 0.7 h; various Ni-ligand with π-acidic P ligands; MechanismProduct distribution;
参考文献
Leeuwen, P. W. N. M. van; Roobeek, C. F.
Tetrahedron, 1981 , vol. 37, p. 1973 - 1984
反应条件
bis(acetylacetonate)nickel(II); SCl2; diisobutylaluminium hydride
1) hexane, 5 deg C, 20 h, 2) toluene, r.t., 2 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tolstikov, G. A.; Lerman, B. M.; Komissarova, N. G.; Zelenova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 283 - 291
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 321 - 332