(3-溴丙基)(苯基甲基)氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
triethylamine in methanol T=20°C; 1 h;
参考文献
Gahman, Timothy C.; Herbert, Mark R.; Lang, Henk; Thayer, Angie; Symons, Kent T.; Nguyen, Phan Manh; Massari, Mark E.; Dozier, Sara; Zhang, Yan; Sablad, Marciano; Rao, Tadimeti S.; Noble, Stewart A.; Shiau, Andrew K.; Hassig, Christian A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 22 p. 6888 - 6894
反应条件
1: sodium tris(acetoxy)borohydride; acetic acid / isopropyl alcohol / 3 h / 20 °C 2: triethylamine / methanol / 1 h / 20 °C View Scheme
参考文献
Gahman, Timothy C.; Herbert, Mark R.; Lang, Henk; Thayer, Angie; Symons, Kent T.; Nguyen, Phan Manh; Massari, Mark E.; Dozier, Sara; Zhang, Yan; Sablad, Marciano; Rao, Tadimeti S.; Noble, Stewart A.; Shiau, Andrew K.; Hassig, Christian A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 22 p. 6888 - 6894
反应条件
1: s-BuLi/(-)sparteine / toluene / -78 °C 2: 86 percent / trifluoroacetic acid / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Wu; Lee; Beak
Journal of the American Chemical Society, 1996 , vol. 118, # 4 p. 715 - 721
反应条件
sec.-butyllithium; (-)-sparteine in toluene T=-78°C; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 118, # 4 p. 715 - 721
