2,3,5,6-四甲基苯甲醛合成路线 （共 18 条）
反应条件
2-nitropropane sodium salt in ethanol
参考文献
Bastianelli, Carlo; Caia, Vincenzo; Cum, Giampietro; Gallo, Raffaele; Mancini, Vittorio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 5 p. 679 - 683
反应条件
titanium tetrachloride in dichloromethane Ambient temperature;
参考文献
Yakubov, Alexander P.; Tsyganov, Dmitry V.; Belen'kii, Leonid I.; Krayushkin, Mikhail M.
Tetrahedron, 1993 , vol. 49, # 16 p. 3397 - 3404
反应条件
1: 1,4-dichloro-2,3,5,6-tetramethylbenzene With naphthalene; lithium in diethyl ether T=20°C; 4 h; 2: N,N-dimethyl-formamide in diethyl ether T=20°C; Cooling with ice;
参考文献
Organic Letters, , vol. 14, # 22 p. 5680 - 5683
反应条件
titanium tetrachloride in dichloromethane T=0°C;
参考文献
Organic Mass Spectrometry, , vol. 23, p. 42 - 47
反应条件
AlCl3, aluminium chloride in nitromethane; dichloromethane T=0°C;
参考文献
WO2004/41752 A2, ;
Page 10 ;
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 8 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
