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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
174390-08-0
合成路线
（共 7 条）
174390-08-0
→
反应条件
106-02-5
环十五内酯
反应条件
copper diacetate in butan-1-ol T=115 - 116°C; Decomposition; 2 h;
参考文献
Ogibin; Terent'ev; Nikishin
Russian Chemical Bulletin, 1998 , vol. 47, # 6 p. 1166 - 1169
174390-08-0
→
反应条件
106-02-5
环十五内酯
+
4941-78-0
氧杂环十六碳-13-烯-2-酮
+
32539-78-9
反应条件
sodium hydroxide; copper diacetate in polydiol; water; propionic acid T=90°C; 3 h; Product distribution / selectivity;
参考文献
Lambrecht, Stefan; Marks, Werner; Topp, Hans-Juergen; Richter, Norbert; Kuhn, Walter
Patent: US2005/85536 A1, 2005 ;
Location in patent: Page/Page column 4 ;
174390-08-0
→
反应条件
106-02-5
环十五内酯
+
4941-78-0
氧杂环十六碳-13-烯-2-酮
+
32539-78-9
反应条件
sodium hydroxide; copper diacetate in polydiol; water; propionic acid T=90°C; 3 h; Product distribution / selectivity;
参考文献
Lambrecht, Stefan; Marks, Werner; Topp, Hans-Juergen; Richter, Norbert; Kuhn, Walter
Patent: US2005/85536 A1, 2005 ;
Location in patent: Page/Page column 4 ;
174390-08-0
→
反应条件
32539-78-9
+
76293-72-6
反应条件
1: With PEG400; isobutyl methylketone; copper diacetate T=85 - 118°C; P=412.541 Torr; 0.5 h; Heating / reflux; 2: 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane in water T=0 - 90°C; P=262.526 Torr; Product distribution / selectivity;
参考文献
Symrise GmbH and Co. KG
Patent: EP1375491 A1, 2004 ;
Location in patent: Page/Page column 7-8 ;
174390-08-0
→
反应条件
32539-78-9
+
76293-72-6
反应条件
1: With PEG400; isobutyl methylketone; copper diacetate T=85 - 118°C; P=412.541 Torr; 0.5 h; Heating / reflux; 2: 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane in water T=0 - 90°C; P=262.526 Torr; Product distribution / selectivity;
参考文献
Symrise GmbH and Co. KG
Patent: EP1375491 A1, 2004 ;
Location in patent: Page/Page column 7-8 ;
174390-08-0
→
反应条件
32539-78-9
+
76293-72-6
反应条件
1: With PEG400; isobutyl methylketone; copper diacetate T=85 - 118°C; P=412.541 Torr; 0.5 h; Heating / reflux; 2: 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane in water T=0 - 90°C; P=262.526 Torr; Product distribution / selectivity;
参考文献
Symrise GmbH and Co. KG
Patent: EP1375491 A1, 2004 ;
Location in patent: Page/Page column 7-8 ;
174390-08-0
→
反应条件
106-02-5
环十五内酯
+
4941-78-0
氧杂环十六碳-13-烯-2-酮
+
32539-78-9
反应条件
sodium hydroxide; copper diacetate in polydiol; water; propionic acid T=90°C; 3 h; Product distribution / selectivity;
参考文献
Lambrecht, Stefan; Marks, Werner; Topp, Hans-Juergen; Richter, Norbert; Kuhn, Walter
Patent: US2005/85536 A1, 2005 ;
Location in patent: Page/Page column 4 ;
