反应条件
in tetrahydrofuran
under Ar, THF soln. of (DCPE)NiCl2 frozen by liquid N2, addn. of (CH3)3SiPH2, mixt. warmed to -20°C and stirred for 12 h; volume reduced in vac. at -20°C, cooled for 24 h at -78°C, pptn., filtration at -20°C, dried in vac. at -20°C;
参考文献
Schaefer, H.; Binder, D.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 557, p. 45 - 58
