trichlorosilane; N,N-dimethyl-aniline in toluene Heating;

<b>Multi-step reaction with 3 steps<br /> </b>1.1: isopropylmagnesium chloride lithium chloride complex / diethyl ether; tetrahydrofuran / 0.5 h / -78 &deg;C / |Inert atmosphere; |Schlenk technique<br />1.2: 2 h / -78 - 20 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.1: hydrogen peroxide / dichloromethane; water / 3 h / 0 &deg;C<br />3.1: copper(l) chloride / DMFA / 3 h / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '706446', constants.ctx, '0')">1,4-di(diphenylphosphino)-butane</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '11324644', constants.ctx, '0')">palladium diacetate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '506008', constants.ctx, '0')">dimethyl sulfoxide</a> <br />T=100&deg;C;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 1.) phenyllithium, lithium bromide, 2.) iodine / 1.) diethyl ether, -25 deg C, 72 h; 2.) diethyl ether<br />2: 78 percent / activated copper / dimethylformamide / 48 h / Heating<br /> <br /> &nbsp;

<b>Multi-step reaction with 4 steps<br /> </b>1.1: 3 h / 20 &deg;C<br />2.1: isopropylmagnesium chloride lithium chloride complex / diethyl ether; tetrahydrofuran / 0.5 h / -78 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.2: 2 h / -78 - 20 &deg;C / |Inert atmosphere; |Schlenk technique<br />3.1: hydrogen peroxide / dichloromethane; water / 3 h / 0 &deg;C<br />4.1: copper(l) chloride / DMFA / 3 h / 20 &deg;C<br /> <br /> &nbsp;