6,7-二甲氧基-1,2,3,4-四氢异喹啉合成路线 （共 60 条）
反应条件
benzophenone in benzene 24 h; Irradiation;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 5 p. 525 - 526
反应条件
polymer-supported S-nitroso-N-acetylpenicillamine in dichloromethane
140 h;
参考文献
Roche, Didier; Lardy, Claude; Tournier, Lucie; Prunier, Marc; Valeur, Eric
Tetrahedron Letters, 2010 , vol. 51, # 17 p. 2277 - 2280
反应条件
in ethyl acetate
T=0 - 20°C;
参考文献
Molander, Gary A.; Pack, Shawn K.
Tetrahedron, 2003 , vol. 59, # 52 p. 10581 - 10591
反应条件
potassium hydride; triethylamine in ethylene glycol dimethyl ether
2 h; Ambient temperatureother alkyl halides; var. bases, excess halide scavenger and time; Product distribution;
参考文献
Mohri; Suzuki; Usui; Isobe; Tsuda
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 1 p. 159 - 161
反应条件
potassium phosphate buffer; sodium L-ascorbate; coclaurine N-methyltransferase in water
T=30°C; pH=7.0; 1 h; Kinetics; Further Variations:relative activity (vs (S)-coclaurine);
参考文献
Choi, Kum-Boo; Morishige, Takashi; Sato, Fumihiko
Phytochemistry, 2001 , vol. 56, # 7 p. 649 - 655
反应条件
potassium hydride; triethylamine
1.) DME, 0 deg C, 0.5 h, 2.) DME, RT, 2 h; Yield given. Multistep reaction;
参考文献
Mohri; Suzuki; Usui; Isobe; Tsuda
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 1 p. 159 - 161
反应条件
1: H+ / 150 °C
2: 48 percent / ZnCl2 / N,N-dimethyl-acetamide / 2 h / Heating
View Scheme
参考文献
Campbell, Simon F.; Hardstone, J. David; Palmer, Michael, J.
Tetrahedron Letters, 1984 , vol. 25, # 42 p. 4813 - 4816
反应条件
chromium(VI) oxide; sulfuric acid
T=0°C;
参考文献
Ahl; Reichstein
Helvetica Chimica Acta, 1944 , vol. 27, p. 366,374
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in acetonitrile
T=0 - 20°C; 2 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
1: 92 percent / iodosylbenzene / tetrabutylammonium iodide / acetonitrile / 0.25 h / 0 °C
2: iodosylbenzene; [Bu4N]I / acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
