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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-苯并呋喃甲腈
合成路线
（共 6 条）
1430837-12-9
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
1: With copper(l) iodide; triethylamine in ethanol T=75°C; 6.5 h; 2: With sodium carbonate; sodium hydroxide in chloroform 18 h;
参考文献
Williams, John D.; Ding, Xiaoyuan; Nguyen, Son; Vines, Kimberly K.; Peet, Norton P.
Synthetic Communications, 2013 , vol. 43, # 14 p. 1974 - 1979
748101-41-9
+
227752-25-2
苯并呋喃-6-基 三氟甲烷磺酸
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=100°C;
参考文献
Nguyen, Son T.; Williams, John D.; Majgier-Baranowska, Helena; Li, Bing; Neelagiri, Venugopal R.; Kim, Hwa-Ok; Peet, Norton P.
Synthetic Communications, 2014 , vol. 44, # 9 p. 1307 - 1313
1430837-12-9
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
copper(l) iodide; triethylamine in ethanol T=50°C; 5 h; TemperatureTime; Overall yield = 94 percent;
参考文献
Williams, John D.; Ding, Xiaoyuan; Nguyen, Son; Vines, Kimberly K.; Peet, Norton P.
Synthetic Communications, 2013 , vol. 43, # 14 p. 1974 - 1979
873-62-1
3-氰基苯酚
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
1.1: sodium iodide; sodium carbonate; iodine / water / 2 h 2.1: water; 4-methyl-morpholine / 24 h / |Reflux 3.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran; chloroform / 3 h / 50 °C 4.1: triethylamine; copper(l) iodide / ethanol / 6.5 h / 75 °C 4.2: 18 h View Scheme
参考文献
Williams, John D.; Ding, Xiaoyuan; Nguyen, Son; Vines, Kimberly K.; Peet, Norton P.
Synthetic Communications, 2013 , vol. 43, # 14 p. 1974 - 1979
6272-26-0
6-羟基-2H-苯并呋喃-3-酮
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
1: lithium borohydride / tetrahydrofuran 2: borane-THF / tetrahydrofuran 3: pyridine; dichloromethane 4: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 100 °C View Scheme
参考文献
Nguyen, Son T.; Williams, John D.; Majgier-Baranowska, Helena; Li, Bing; Neelagiri, Venugopal R.; Kim, Hwa-Ok; Peet, Norton P.
Synthetic Communications, 2014 , vol. 44, # 9 p. 1307 - 1313
1020947-92-5
→
反应条件
17450-68-9
6-苯并呋喃甲腈
反应条件
1: borane-THF / tetrahydrofuran 2: pyridine; dichloromethane 3: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 100 °C View Scheme
参考文献
Nguyen, Son T.; Williams, John D.; Majgier-Baranowska, Helena; Li, Bing; Neelagiri, Venugopal R.; Kim, Hwa-Ok; Peet, Norton P.
Synthetic Communications, 2014 , vol. 44, # 9 p. 1307 - 1313
