1-丁基-3-甲基咪唑六氟磷酸盐合成路线 （共 24 条）
反应条件
1: 60 - 70 °C 2: NH4PF6 View Scheme
参考文献
Chemical Communications, , # 5 p. 590 - 591
反应条件
1: potassium fluoride; N-trimethylsilyl-tris(pentafluorethyl)phosphazen; boric acid trimethyl ester in ethylene glycol dimethyl ether T=20 - 60°C; 1 h; 2: hydrogen fluoride in ethylene glycol dimethyl ether; water T=0 - 20°C; 3 h; 3: 1-n-butyl-3-methylimidazolium chloride in water
参考文献
WO2005/105815 A1, ;
Page/Page column 15-17 ;
反应条件
alkali metal hexafluorophosphate T=150°C; 0.5 h; Microwave irradiationCoolingneat (no solvent);
参考文献
Combinatorial Chemistry and High Throughput Screening, , vol. 15, # 5 p. 427 - 432
反应条件
in water T=20°C; 24 h;
参考文献
Advanced Materials, , vol. 24, # 45 p. 6081 - 6087
参考文献
US6339182 B1, ;
Table 1 ;
参考文献
Meine, Niklas; Benedito, Flavio; Rinaldi, Roberto
Green Chemistry, 2010 , vol. 12, # 10 p. 1711 - 1714
反应条件
1: Rh(acac)(CO)2; 1-n-butyl-3-methylimidazolium hexafluorophosphate; sulfoxantphos With carbon monoxide; hydrogen in anhydrous butyl ether T=120°C; P=8250.83 Torr; 0.5 h; 2: oct-1-ene P=8250.83 Torr; 2 h; Conversion of starting material;
参考文献
Bohnen, Hans; Herwig, Jurgen; Hoff, Dietmar; Wasserscheid, Peter; Hal, Roy van
Patent: US2005/85671 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
cesium fluoride T=150°C; 96 h;
参考文献
Murray, Christopher B.; Sandford, Graham; Korn, Stewart R.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 1 p. 81 - 84
参考文献
Meine, Niklas; Benedito, Flavio; Rinaldi, Roberto
Green Chemistry, 2010 , vol. 12, # 10 p. 1711 - 1714
反应条件
oxygen in dichloromethane not isolated;
参考文献
Choi, Doo Seong; Kim, Dong Hyun; Shin, Ueon Sang; Deshmukh, Ravindra R.; Lee, Sang-Gi; Song, Choong Eui
Chemical Communications, 2007 , # 33 p. 3467 - 3469
