1-丁基-3-甲基咪唑四氟硼酸盐合成路线 （共 45 条）
反应条件
NH4BF4 in water T=20°C; 2 h;
参考文献
Gauchot, Vincent; Kroutil, Wolfgang; Schmitzer, Andreea R.
Chemistry - A European Journal, 2010 , vol. 16, # 23 p. 6748 - 6751
反应条件
sodium tetrafluoroborate T=70°C; 336 h;
参考文献
Solvent Innovation GmbH
Patent: EP1182197 A1, 2002 ;
Location in patent: Page 9 ;
反应条件
sodium tetrafluoroborate T=80°C; 3.5 h;
参考文献
Fang, Dong; Cheng, Jian; Gong, Kai; Shi, Qun-Rong; Zhou, Xin-Li; Liu, Zu-Liang
Journal of Fluorine Chemistry, 2008 , vol. 129, # 2 p. 108 - 111
反应条件
1: in methanol T=135°C; 7 h; 2: With tetrafluoroboric acid in diethyl ether 2 h;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: EP1398318 A1, 2004 ;
Location in patent: Page 17 ;
反应条件
triethylsulfonium tetrafluoroborate in dichloromethane T=60 - 70°C; 672 h; Product distribution / selectivity;
参考文献
MERCK PATENT GMBH
Patent: WO2006/7912 A1, 2006 ;
Location in patent: Page/Page column 19-20 ;
反应条件
1: 0.25 h; 2: With sodium tetrafluoroborate in water
参考文献
Solvent Innovation GmbH
Patent: EP1182196 A1, 2002 ;
Location in patent: Page 10, 11 ;
反应条件
Amberlist A-26 BF4(-) form in methanol Ionic liquid;
参考文献
Alcalde, Ermitas; Dinares, Immaculada; Ibanez, Anna; Mesquida, Neus
Molecules, 2012 , vol. 17, # 4 p. 4007 - 4027
反应条件
tetrafluoroboric acid in water T=25°C; 0.5 h;
参考文献
BASF Aktiengesellschaft
Patent: WO2006/27070 A1, 2006 ;
Location in patent: Page/Page column 30-31 ;
反应条件
in acetone react. of equal moles of (C3H3N2CH3C4H9)Cl with NaBF4 in acetone; stirring at room temp. for 24 h; filtering and vac. drying overnight at 50°C; detd. by NMR;
参考文献
Xiao, Li; Johnson, Keith E.
Journal of the Electrochemical Society, 2003 , vol. 150, # 6 p. E307-E311
反应条件
sodium tetrafluoroborate in tetrahydrofuran T=20°C; 70 h;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 2141 - 2145
