3-溴-4,5,6,7-四氢-7-氧代-1H-吲哚-2-羧酸乙酯合成路线 （共 5 条）
反应条件
pyridine; pyridinium hydrobromide perbromide T=0°C; 0.4 h;
参考文献
Tani, Masanobu; Ariyasu, Takahiro; Ohtsuka, Masanori; Koga, Terumi; Ogawa, Yumi; Yokoyama, Yuusaku; Murakami, Yasuoki
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 55 - 61
反应条件
1: 87 percent / aluminum chloride / 1,2-dichloro-ethane / 2 h / Ambient temperature 2: triethylsilane, trifluoroacetic acid / 25 h / Ambient temperature 3: trifluoroacetic acid, trifluoroacetic anhydride / 1 h / Ambient temperature 4: 92 percent / pyridinium bromide perbromide, pyridine / 0.4 h / 0 °C View Scheme
参考文献
Tani, Masanobu; Ariyasu, Takahiro; Ohtsuka, Masanori; Koga, Terumi; Ogawa, Yumi; Yokoyama, Yuusaku; Murakami, Yasuoki
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 55 - 61
反应条件
1: 94 percent / AcOH, 30percent aq. H2SO4 / 0.33 h / 100 °C 2: trifluoroacetic acid, trifluoroacetic anhydride / 1 h / Ambient temperature 3: 92 percent / pyridinium bromide perbromide, pyridine / 0.4 h / 0 °C View Scheme
参考文献
Tani, Masanobu; Ariyasu, Takahiro; Ohtsuka, Masanori; Koga, Terumi; Ogawa, Yumi; Yokoyama, Yuusaku; Murakami, Yasuoki
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 55 - 61
反应条件
1: 91.6 percent / triethylsilane, trifluoroacetic acid / 24 h / Ambient temperature 2: 94 percent / AcOH, 30percent aq. H2SO4 / 0.33 h / 100 °C 3: trifluoroacetic acid, trifluoroacetic anhydride / 1 h / Ambient temperature 4: 92 percent / pyridinium bromide perbromide, pyridine / 0.4 h / 0 °C View Scheme
参考文献
Tani, Masanobu; Ariyasu, Takahiro; Ohtsuka, Masanori; Koga, Terumi; Ogawa, Yumi; Yokoyama, Yuusaku; Murakami, Yasuoki
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 55 - 61
反应条件
1: trifluoroacetic acid, trifluoroacetic anhydride / 1 h / Ambient temperature 2: 92 percent / pyridinium bromide perbromide, pyridine / 0.4 h / 0 °C View Scheme
参考文献
Tani, Masanobu; Ariyasu, Takahiro; Ohtsuka, Masanori; Koga, Terumi; Ogawa, Yumi; Yokoyama, Yuusaku; Murakami, Yasuoki
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 55 - 61
