1-Cbz-3-甲基哌啶-3-羧酸甲酯合成路线 （共 5 条）
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Taylor, G. Mark; Baker, Stewart J.; Gedney, Andrea; Pearson, David J.; Sibley, Graham E. M.
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1297 - 1300
反应条件
N,N'-dimethyl-N,N'-propyleneurea; lithium hexamethyldisilazane in tetrahydrofuran
T=-60°C; to room temperature;
参考文献
Taylor, G. Mark; Baker, Stewart J.; Gedney, Andrea; Pearson, David J.; Sibley, Graham E. M.
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1297 - 1300
反应条件
1: HCl
2: 90 percent / LiN(TMS)2, DMPU / tetrahydrofuran / -60 °C / to room temperature
View Scheme
参考文献
Taylor, G. Mark; Baker, Stewart J.; Gedney, Andrea; Pearson, David J.; Sibley, Graham E. M.
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1297 - 1300
反应条件
1: 98 percent / NaHCO3 / dioxane
2: HCl
3: 90 percent / LiN(TMS)2, DMPU / tetrahydrofuran / -60 °C / to room temperature
View Scheme
参考文献
Taylor, G. Mark; Baker, Stewart J.; Gedney, Andrea; Pearson, David J.; Sibley, Graham E. M.
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1297 - 1300
反应条件
1: 98 percent / NaHCO3 / dioxane
2: HCl
3: 90 percent / LiN(TMS)2, DMPU / tetrahydrofuran / -60 °C / to room temperature
View Scheme
参考文献
Taylor, G. Mark; Baker, Stewart J.; Gedney, Andrea; Pearson, David J.; Sibley, Graham E. M.
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1297 - 1300
