N,N-二甲基-4-硝基苯磺酰胺合成路线 (共 6 条)
反应条件
hydrogen; palladium on carbon in methanol
参考文献
WO2011/19405 A1, ;
Page/Page column 101-102 ;
WO 2011/019405 A1
反应条件
in tetrahydrofuran
T=0 - 20°C; 2 h;
参考文献
RIB-X PHARMACEUTICALS, INC.
Patent: WO2004/29066 A2, 2004 ;
Location in patent: Page/Page column 312 ;
参考文献
BIOLIPOX AB
Patent: WO2007/51982 A1, 2007 ;
Location in patent: Page/Page column 41 ;
反应条件
dimethyl amine in methanol; water
参考文献
Eli Lilly and Company
Patent: US6635657 B1, 2003 ;
US 6635657 B1
反应条件
aluminum oxide; potassium hydroxide
T=130°C; 0.0666667 h; microwave irradiation;
参考文献
Malik, Sarika; Nadir, Upender K.; Pandey, Pramod S.
Synthetic Communications, 2008 , vol. 38, # 18 p. 3074 - 3081
反应条件
copper diacetate; 3-phenyl-2-propenoic acid; copper(l) chloride
T=110°C; 24 h;
参考文献
Huang, Xin; Wang, Jichao; Ni, Zhangqin; Wang, Sichang; Pan, Yuanjiang
Chemical Communications, 2014 , vol. 50, # 35 p. 4582 - 4584