2-[(1R,2S,3R)-1,2,3,4-羟基丁基]-5-[(2S,3R)-2,3,4-三羟基丁基]吡嗪合成路线 (共 6 条)
反应条件
sodium hydroxide; 3,4,5-trimethoxyphenylboronic acid T=20°C; 3 h;
参考文献
Rohovec, Jan; Kotek, Jan; Peters, Joop A.; Maschmeyer, Thomas
European Journal of Organic Chemistry, 2001 , # 20 p. 3899 - 3901
反应条件
pyridine; L-cysteine monohydrochloride powder in methanol; water 32 h; Heating;
参考文献
Sumoto; Irie; Mibu; Miyano; Nakashima; Watanabe; Yamaguchi
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 792 - 794
反应条件
ammonium hydroxide in water 504 h; Ambient temperature;
参考文献
Sumoto; Irie; Mibu; Miyano; Nakashima; Watanabe; Yamaguchi
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 792 - 794
反应条件
diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; sodium phosphate buffer; oxygen T=37°C; pH=7.4; 24 h;
参考文献
Shimamura, Tomoko; Takamori, Atsuko; Ukeda, Hiroyuki; Sawamura, Masayoshi
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 2 p. 295 - 299
反应条件
DAHP in water T=93°C; pH=8.0; 2.5 h; Product distribution; Further Variations:Reagents;
参考文献
Agyei-Aye, Kwasi; Chian, May X; Lauterbach, John H; Moldoveanu, Serban C
Carbohydrate Research, 2002 , vol. 337, # 21-23 p. 2273 - 2277
反应条件
T=130°C; 4.5 h; Te buffer; other solvents other temperatures, other times, other pH; Product distribution;
参考文献
Sumoto; Irie; Mibu; Miyano; Nakashima; Watanabe; Yamaguchi
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 792 - 794