potassium hydroxide in methanol; water 1 h; Ambient temperature;
参考文献
Rewcastle, Gordon W.; Palmer, Brian D.; Bridges, Alexander J.; Showalter, H.D. Hollis; Sun, Li; Nelson, James; McMichael, Amy; Kraker, Alan J.; Fry, David W.; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 4 p. 918 - 928
1: 98 percent / ethanol; H2O / 2 h / 100 °C 2: 1.) H2, HCOOH / 1.) 5percent Pd/C / 1.) C2H5OH, 20 deg C, 2.) reflux, 2 h 3: 59 percent / P2S5, pyridine / 16 h / Heating 4: 54 percent / KOH / methanol; H2O / 1 h / Ambient temperature View Scheme
参考文献
Rewcastle, Gordon W.; Palmer, Brian D.; Bridges, Alexander J.; Showalter, H.D. Hollis; Sun, Li; Nelson, James; McMichael, Amy; Kraker, Alan J.; Fry, David W.; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 4 p. 918 - 928
Rewcastle, Gordon W.; Palmer, Brian D.; Bridges, Alexander J.; Showalter, H.D. Hollis; Sun, Li; Nelson, James; McMichael, Amy; Kraker, Alan J.; Fry, David W.; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 4 p. 918 - 928
1: 59 percent / P2S5, pyridine / 16 h / Heating 2: 54 percent / KOH / methanol; H2O / 1 h / Ambient temperature View Scheme
参考文献
Rewcastle, Gordon W.; Palmer, Brian D.; Bridges, Alexander J.; Showalter, H.D. Hollis; Sun, Li; Nelson, James; McMichael, Amy; Kraker, Alan J.; Fry, David W.; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 4 p. 918 - 928
