1-(2-氯-苯基)-3,4-二氢-异喹啉合成路线 (共 6 条)
反应条件
sodium hydroxide in water; dimethyl sulfoxide T=70°C; 1.5 h; regiospecific reaction;
参考文献
Dong, Jing; Shi, Xiao-Xin; Xing, Jing; Yan, Jing-Jing
Synthetic Communications, 2012 , vol. 42, # 19 p. 2806 - 2817
反应条件
phosphorus pentoxide in xylene Dehydration; cyclization; Heating;
参考文献
Suna; Trapencieris
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 3 p. 287 - 300
反应条件
1: 92.9 percent / triethylamine / CH2Cl2 / 3 h / 20 °C 2: phosphorus oxychloride / toluene / 8 h / Heating View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
反应条件
1: thionyl chloride / CH2Cl2 / 0 - 20 °C 2: 92.9 percent / triethylamine / CH2Cl2 / 3 h / 20 °C 3: phosphorus oxychloride / toluene / 8 h / Heating View Scheme
参考文献
Suna; Trapencieris
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 3 p. 287 - 300
反应条件
1: triethylamine / acetonitrile / 2 h 2: POCl3 / acetonitrile / 3 h / Heating View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
反应条件
manganese(IV) oxide in benzene
96 h; Heating;
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532