1-正丁基-3-甲基咪唑三氟甲烷磺酸盐合成路线 （共 19 条）
参考文献
Ignat'ev, Nikolai V.; Barthen, Peter; Kucheryna, Andryi; Willner, Helge; Sartori, Peter
Molecules, 2012 , vol. 17, # 5 p. 5319 - 5338
反应条件
1: 0.25 h; 2: With sodium trifluoro-methanesulfonate in water
参考文献
Solvent Innovation GmbH
Patent: EP1182196 A1, 2002 ;
Location in patent: Page 14 ;
反应条件
1: in dichloromethane T=0 - 20°C; 1 h; 2: With sodium carbonate in dichloromethane; water T=20°C; 0.5 h; Product distribution / selectivity;
参考文献
PETROLEO BRASILEIRO S.A. - PETROBRAS
Patent: US2008/45723 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
1: CF3O3S(1-)*H(1+)*H3N With Amberlyst A-26 (OH- form) in water T=20°C; 2: [bmim][I] in methanol
参考文献
Alcalde, Ermitas; Dinares, Immaculada; Ibanez, Anna; Mesquida, Neus
Molecules, 2012 , vol. 17, # 4 p. 4007 - 4027
反应条件
1: trifluorormethanesulfonic acid With sodium hydroxide in water pH=6 - 7; cooling; 2: [N-butylthiazolium][OMs] in water 0.5 h;
参考文献
Cassol, Claudia C.; Ebeling, Guenter; Ferrera, Bauer; Dupont, Jairton
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 1-2 p. 243 - 248
反应条件
in neat (no solvent) T=100°C; 0.333333 h; Microwave irradiation;
参考文献
Hoangtran, Phuong; Bichle Do, Ngoc; Ngocle, Thach
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 205 - 208
反应条件
in water T=20°C; 6 h;
参考文献
Deng, Hui; Li, Xin; Chu, Yuan; He, Jiaqi; Cheng, Jin-Pei
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7291 - 7298
反应条件
in acetonitrile Heating;
参考文献
Xu, Wu; Wang, Li-Min; Nieman, Ronald A.; Angell, C. Austen
Journal of Physical Chemistry B, 2003 , vol. 107, # 42 p. 11749 - 11756
反应条件
T=45 - 120°C; 0.166667 h; microwave irradiation; sonication;
参考文献
Cravotto, Giancarlo; Boffa, Luisa; L'Eveque, Jean-Marc; Estager, Julien; Draye, Micheline; Bonrath, Werner
Australian Journal of Chemistry, 2007 , vol. 60, # 12 p. 946 - 950
反应条件
1.1: 96 percent / 24 h / 20 °C 2.1: NaOH / H2O / pH 6 - 7 / cooling 2.2: 92 percent / H2O / 0.5 h View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 1-2 p. 243 - 248
