N-(4-甲氧基亚苄基)-4-甲氧基苯胺合成路线 (共 19 条)
反应条件
1.1: potassium hydroxide / N,N-dimethyl-formamide / 1 h / 120 °C 1.2: 5 h / 120 °C 2.1: ethanol View Scheme
参考文献
Wu, Yiran; Chen, Zheng; Liu, Ying; Yu, Lanlan; Zhou, Lu; Yang, Suijia; Lai, Luhua
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3361 - 3366
反应条件
in tetrahydrofuran T=55°C; 3 h; Further byproducts given;
参考文献
Okubo, Masao; Yoshida, Shunsei; Egami, Yoshiji; Matsuo, Koji; Nagase, Shigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1741 - 1746
反应条件
in tetrahydrofuran T=55°C; 3 h; Product distributionMechanism;
参考文献
Okubo, Masao; Yoshida, Shunsei; Egami, Yoshiji; Matsuo, Koji; Nagase, Shigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1741 - 1746
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in toluene T=70°C; 24 h; Inert atmosphere;
参考文献
Li, Jianhui; Wang, Zhouyu; Jiang, Zhenju; Jiang, Shengqian; Xiong, Lilin
Asian Journal of Chemistry, 2011 , vol. 23, # 9 p. 4101 - 4103
反应条件
boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid in water T=0°C; 6 h;
参考文献
An, Gwang-Il; Kim, Misoo; Kim, Jin Yeon; Rhee, Hakjune
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2183 - 2186
反应条件
H-Y (SiO2/Al2O3 = 5.6) zeolite T=60°C; Aza-Henry reaction; 9 h;
参考文献
Applied Catalysis A: General, , vol. 388, # 1-2 p. 211 - 215
反应条件
acetic acid Heating; Yield given;
参考文献
Singh, Harjit; Sarin, Rakesh
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2623 - 2640
反应条件
in tetrahydrofuran T=70°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Shao, You-Dong; Wu, Xue-Song; Tian, Shi-Kai
European Journal of Organic Chemistry, 2012 , # 8 p. 1590 - 1596
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane
T=50°C; 2 h;
参考文献
Tewari, Ram S.; Awasthi, Alok K.; Awasthi, Anita
Synthesis, 1983 , # 4 p. 330 - 331