苯基-(1-苯亚乙基)胺合成路线 （共 42 条）
反应条件
1: 200 - 210 °C 2: potassium hydroxide; water / 250 - 260 °C View Scheme
参考文献
Dziewonski; Moszew
Roczniki Chemii, 1932 , vol. 12, p. 482,490
Chem. Zentralbl., 1932 , vol. 103, # II p. 3401
反应条件
1: N-chlorosuccinimide / CCl4 / 1.) heating, 1-2 min, 2.) 10 deg C, 1 h 2: 66 percent / lithium aluminium hydride / diethyl ether / 1 h / Heating View Scheme
参考文献
Kimpe, Norbert De; Verhe, Roland; Buyck, Laurent De; Schamp, Niceas
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2079 - 2081
反应条件
sulfur T=220 - 240°C;
参考文献
Bogert; Herrera
Journal of the American Chemical Society, 1923 , vol. 45, p. 240
反应条件
1: potassium hydride / tetrahydrofuran / 50 °C / Inert atmosphere 2: water View Scheme
参考文献
Kutlescha, Kathrin; Venkanna, Gopaladasu T.; Kempe, Rhett
Chemical Communications, 2011 , vol. 47, # 14 p. 4183 - 4185
反应条件
Co(II) complex supported on mesoporous SBA-15 T=40°C; Strecker-type reaction; 10 h;
参考文献
Rajabi, Fatemeh; Nourian, Saghar; Ghiassian, Sara; Balu, Alina M.; Saidi, Mohammad Reza; Serrano-Ruiz, Juan Carlos; Luque, Rafael
Green Chemistry, 2011 , vol. 13, # 11 p. 3282 - 3289
反应条件
tris(dibenzylideneacetone)dipalladium (0); lithium tert-butylate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
Barluenga, Jose; Jimenez-Aquino, Agustin; Aznar, Fernando; Valdes, Carlos
Journal of the American Chemical Society, 2009 , vol. 131, p. 4031 - 4041
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutylammomium bromide; potassium hydroxide; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=140°C; 0.75 h; Microwave irradiation;
参考文献
Barluenga, Jose; Jimenez-Aquino, Agustin; Aznar, Fernando; Valdes, Carlos
Chemistry - A European Journal, 2010 , vol. 16, # 38 p. 11707 - 11711
反应条件
tris(dibenzylideneacetone)dipalladium (0); lithium tert-butylate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=110°C; 14 h; Inert atmosphere;
参考文献
Barluenga, Jose; Jimenez-Aquino, Agustin; Aznar, Fernando; Valdes, Carlos
Journal of the American Chemical Society, 2009 , vol. 131, p. 4031 - 4041
反应条件
tris(dibenzylideneacetone)dipalladium (0); sodium t-butanolate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=110°C; 14 h; Inert atmosphere;
参考文献
Barluenga, Jose; Jimenez-Aquino, Agustin; Aznar, Fernando; Valdes, Carlos
Journal of the American Chemical Society, 2009 , vol. 131, p. 4031 - 4041
参考文献
Reddelien
Chemische Berichte, 1913 , vol. 46, p. 2720
Chemische Berichte, 1915 , vol. 48, p. 1469
